Preparation of Ultrafine Cobalt Ferrite Particles by Solution SHS Method | |
Li, Xi-en; Zhu, Xuhua | |
2011 | |
会议名称 | MATERIALS AND DESIGN, PTS 1-3 |
会议录名称 | TRANS TECH PUBLICATIONS LTD |
卷号 | 284-286 |
页码 | 645-+ |
会议日期 | JUL 29-31, 2011 |
会议地点 | Sanya, PEOPLES R CHINA |
出版地 | KREUZSTRASSE 10, 8635 DURNTEN-ZURICH, SWITZERLAND |
出版者 | TRANS TECH PUBLICATIONS LTD |
摘要 | Nanosized CoFe2O4 powders of 12nm particle size were directly prepared by solution SHS method at room temperature. The overall process involves three steps: formation of homogeneous sol; formatiom of dried gel; and combustion of the dried gel. Experiments revealed that CoFe2O4 dried gel derived from citrate and nitrate sol exhibited self-propagation combustion(SHS) at room temperature once it was ignited in air. After self-propagating combustion, the gel directly transforms into nanosized CoFe2O4 particles. The self-propagating combustion was considered as a heat-induced exothermic oxidation-reduction reaction between nitrate ions and carboxyl group. Differential thermal analysis-thermogravimetry (DTA-TG) was used to study the decomposition of the precursor. The structure of the nanosized CoFe2O4 powders was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). |
关键词 | CoFe2O4 solution SHS method nanosized powders |
DOI | 10.4028/www.scientific.net/AMR.284-286.645 |
URL | 查看原文 |
收录类别 | CPCI ; CPCI-S |
语种 | 英语 |
WOS研究方向 | Science & Technology - Other Topics ; Materials Science |
WOS类目 | Nanoscience & Nanotechnology ; Materials Science, Ceramics ; Materials Science, Composites |
WOS记录号 | WOS:000302669800128 |
原始文献类型 | Proceedings Paper |
引用统计 | |
文献类型 | 会议论文 |
条目标识符 | http://ir.lzufe.edu.cn/handle/39EH0E1M/9822 |
专题 | 国有资产管理处 基建处 统计与数据科学学院 |
作者单位 | 1.Lanzhou Commercial Coll, Sch Agr & Forestry Econ & Management, Lanzhou 730020, Peoples R China; 2.Lanzhou Commercial Coll, Coll Stat, Lanzhou 730020, Peoples R China |
推荐引用方式 GB/T 7714 | Li, Xi-en,Zhu, Xuhua. Preparation of Ultrafine Cobalt Ferrite Particles by Solution SHS Method[C]. KREUZSTRASSE 10, 8635 DURNTEN-ZURICH, SWITZERLAND:TRANS TECH PUBLICATIONS LTD,2011:645-+. |
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